聚丁二酸丁二醇酯(PBS)制备工艺技术
Preparation Technology of PBS
摘要:
聚丁二酸丁二醇酯(PBS)一般由丁二醇和丁二酸缩聚而得,是典型的可完全降解聚合物材料。本技术采用预缩聚反应和终缩聚反应逐步聚合的新型工艺,该工艺技术包含五大部分:即浆液预制、酯化反应过程、预缩聚反应过程、终缩聚反应过程、干燥过程,该技术工艺流程简单,生产的产品质量标准高、聚合度较高、相对分子质量大,可极大地减低制作成本。
Abstract:
Polybutylene succinate (PBS) is generally obtained by polycondensation of butanediol and succinic acid and is a typical fully degradable polymer material. The technology adopts a novel process of gradual polymerization of pre-polycondensation reaction and final polycondensation reaction, and the process technology comprises five parts: slurry pre-fabrication, esterification reaction process, pre-polycondensation reaction process, final polycondensation reaction process, drying process. This technology has simple process, high product quality standard, high polymerization degree and large relative molecular weight, which can greatly reduce the production cost.
参考文献
|
[1]
|
徐永祥, 徐军, 周啸, 郭宝华, 谢续明. 聚丁二酸丁二酯的多重熔融行为研究[C]//2006年全国高分子材料科学与工程研讨会论文集. 北京: 中国化学会, 2006.
|
|
[2]
|
叶海木, 宋韵洋,王春晓. 聚己二酸丁二酯同质多晶及晶型转变的研究[C]//2015年全国高分子学术论文报告会论文摘要集——主题C高分子物理与软物质. 北京: 中国化学会, 2015.
|
|
[3]
|
张世平, 宫铭, 党媛, 史素青, 宫永宽. 聚丁二酸丁二醇酯的研究进展[J]. 高分子通报, 2011(3).
|