MS  >> Vol. 1 No. 1 (April 2011)

    三角形纳米银粒子的制备及其表征
    Preparation and Characterization of TriangleSilver Nanoparticles

  • 全文下载: PDF(173KB) HTML    PP.7-9   DOI: 10.12677/ms.2011.11002  
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作者:  

代凯,朱光平,刘忠良,刘亲壮,芦露华,陈征

关键词:
三角形制备表征
Triangle; Silver; Preparation; Characterization

摘要:

采用简单液相还原法制备出三角形纳米银粒子。利用透射电子显微镜,选区电子衍射,紫外-可见吸收光谱和X射线衍射对纳米银粒子进行表征。结果表明,该法制备的三角形纳米银粒子杂质含量低,粒度分布集中,颗粒均匀一致,边长约为60~100nm。最后对三角形纳米银的生长机理进行了探讨。

riangle silver (Ag) nanoparticles have been successfully prepared by an easy and large scale productive liquid phase reduction method. The nanosize silver particles were characterized by using transmission electron microscopy (TEM), Selected-area electron diffraction (SAED), UV-Vis absorption spectroscopy and X-ray diffraction (XRD). The results show that the nanosize silver particles produced by this method are pure and spherical with uniform and narrow - dispersed size distribution, the length of a side is about 60 - 100 nm. The mechanism of growth of triangle Ag nanoparticles are dicussed at last.

文章引用:
代凯, 朱光平, 刘忠良, 刘亲壮, 芦露华, 陈征. 三角形纳米银粒子的制备及其表征[J]. 材料科学, 2011, 1(1): 7-9. http://dx.doi.org/10.12677/ms.2011.11002

参考文献

[1] Y. J. Kim, T. S. Shin, and H. D. Choi, et al. Electrical conductivity of chemically modified multiwalled carbon nanotube/epoxy composites. Carbon, 2005, 43(1): 23-30.
[2] M. Yu, H. H. Funke, and J. L. Falconer, et al. Gated ion transport through dense carbon nanotube membranes. Journal of the American Chemical Society, 2010, 132(24): 8285-8290.
[3] 代凯, 施利毅, 方建慧等. 导电胶粘剂的研究进展[J]. 材料导报, 2006, 20(3): 116-118.
[4] K. K. Hong, S. B. Cho, and J. S. You, et al. Mechanism for the formation of Ag crystallites in the Ag thick-film contacts of crystalline Si solar cells. Solar Energy Materials and Solar Cells, 2009, 93(6-7): 898-904.
[5] S. C. Wu, C. F. Chen, and W. C. Chao. Collective optical behavior in complementary wire arrays with Au nanoparticles. Microelectronic Engineering, 2005, 77(3-4): 277-284.
[6] Y. H. Kim, D. K. Lee, and Y. S. Kang. Synthesis and characterization of Ag and Ag–SiO2 nanoparticles. Colloids and Surfaces A: Physicochem. Eng. Aspects, 2005, 257-258(5): 273-276.
[7] R. B. Matthew, A. G. Antonio, and A. H. Steven. A comparison of silver ion to streptavidin coated microplates. Journal of Microbiological Methods, 2001, 44(2): 113-120.
[8] R. Z. Chen, D. S. Xu, and G. L. Guo, et al. Electrodeposition of thin films and single-crystalline nanowires of Ag7Te4 . Chemical Physics Letters, 2003, 377(1-2): 205-209.
[9] Q. Zhang, W. Y. Li, and C. Moran, et al. Seed-Mediated Synthesis of Ag Nanocubes with Controllable Edge Lengths in the Range of 30-200 nm and Comparison of Their Optical Properties. Journal the American Chemical Society, 2010, 132(32): 11372-11378.
[10] A. Filankembo, M. P. Pileni. Shape control of copper nanocrystals. Applied Surface Science, 2000, 164(1-4): 260-267.
[11] A. I. Lukman, B. Gong, and C. E. Marjo, et al. Facile synthesis, stabilization, and anti-bacterial performance of discrete Ag nanoparticles using Medicago sativa seed exudates. Journal of Colloid and Interface Science, 2011, 353(2): 433-444.