二硫化钒–生物质衍生的氮掺杂碳复合纳米材料的制备及储锂性能综合化学实验设计
Design Comprehensive Chemical Experiment on Preparation and Lithium Storage Performance of Vanadium Disulfid-Biomass Derived N-Doped Carbon Nanocomposite
摘要: 新能源和新材料是化学专业的研究重点之一,为了让学生能够更好的学习相关知识,同时考虑到应用化学和材料化学的专业内容,将二硫化钒–生物质衍生的氮掺杂碳复合纳米材料的制备及储锂性能测试简化设计为综合化学实验。实验通过热处理法制备得到多孔二硫化钒复合纳米材料,研究了其作为负极材料时的储锂性能。实验包含基础化学的知识和实验技术,能够帮助学生在巩固学科知识,提高实验技能。同时,实验内容还涉及新材料和新能源的前沿研究,这有助于培养学生的科研能力,为学生后续独立开展工作奠定良好的基础。
Abstract: New energy and new materials is one of the key points of chemistry. In order to allow students to learn related knowledge better, considering the professional content of applied chemistry and material chemistry, preparation and lithium storage performance of vanadium disulfid-biomass derived N-doped carbon nanocomposite was simplified to comprehensive chemical experiment. Heat treatment method is adopted to prepare porous vanadium disulfide nanocomposite. The lithium storage performance of this composite is studied. The experiment including fundamental chemistry and experiment techniques is helpful for students to reinforce the knowledge and improve their experimental skills. At the same time, this experiment which involves the frontier research of new materials and new energy can cultivates students’ scientific research capability and lay a good foundation for students follow-up.
文章引用:孙劲毅, 马琳, 席艳杰, 许丽梅. 二硫化钒–生物质衍生的氮掺杂碳复合纳米材料的制备及储锂性能综合化学实验设计[J]. 创新教育研究, 2022, 10(6): 1375-1384. https://doi.org/10.12677/CES.2022.106221

参考文献

[1] 郭永明. 研究型综合化学实验设计: 碳量子点的制备及其在叶酸检测中的应用[J]. 化学教育(中英文), 2020, 41(16): 29-33.
[2] 章文伟, 张晖, 奚忠华, 孔璇凤. 以“三三制”驱动的综合化学实验课程建设[J]. 实验技术与管理, 2019, 36(8): 218-220, 224.
[3] 朱效华, 陈超, 吴萃艳, 邓文芳, 刘美玲. 科教融合的新型综合化学实验设计[J]. 曲阜师范大学学报(自然科学版), 2021, 47(2): 124-128.
[4] 王薇, 韩帅, 唐晓亮, 郭礼荣, 唐瑜. 牛奶碳量子点的制备与梯度萃取分离——科研转化的综合化学实验[J]. 大学化学, 2021, 36(4): 150-158.
[5] 吴小帅, 杨晓刚, 史转转, 沈杨彬, 郭春显. 协同培养新能源材料与器件特色人才: 以创新力培养为杠杆[J]. 当代化工研究, 2022(5): 105-107.
[6] Li, W., Kheimeh Sari, H.M. and Li, X. (2020) Emerging Layered Metallic Vanadium Disulfide for Rechargeable Metal-Ion Batteries: Progress and Opportunities. ChemSusChem, 13, 1172-1202. [Google Scholar] [CrossRef] [PubMed]
[7] Liu, Y.Y., Xu, L., Guo, X.T., Lv, T.T. and Pang, H. (2020) Vanadium Sulfide Based Materials: Synthesis, Energy Storage and Conversion. Journal of Materials Chemistry A, 8, 20781-20802. [Google Scholar] [CrossRef
[8] Mendoza-Sánchez, B., Coelho, J., Pokle, A. and Nicolosi, V. (2016) A Study of the Charge Storage Properties of a MoSe2 Nanoplatelets/SWCNTs Electrode in a Li-Ion Based Electrolyte. Elec-trochimica Acta, 192, 1-7. [Google Scholar] [CrossRef