Nd-Fe-B磁环反向热挤压成型工艺及性能调控
Tuning of Forming Process and Properties of Backward Hot-Extruded Nd-Fe-B Magnetic Ring
DOI: 10.12677/ms.2024.1412181, PDF,    科研立项经费支持
作者: 郑立允*, 左思源:河北工程大学,稀土永磁材料与应用河北省工程研究中心,河北 邯郸;杜 峰, 李雅婧, 赵立新:河北工程大学,稀土永磁材料与应用河北省工程研究中心,河北 邯郸;河北工程大学,机械与装备工程学院,河北 邯郸;赵树国:邯郸职业技术学院机电工程系,河北 邯郸;方以坤:钢铁研究总院有限公司,功能材料研究院,北京;左志军:廊坊京磁精密材料有限公司,河北 廊坊
关键词: 反向热挤压Nd-Fe-B磁环磁性能凸台结构轴向均匀性Backward Hot-Extrusion Nd-Fe-B Magnetic Ring Magnetic Properties Boss Structure Axial Uniformity
摘要: 采用反向热挤压技术,制备了外径39.5 mm、壁厚4.5 mm的Nd-Fe-B磁环,研究了挤压速度、变形压力和模具结构对反向热挤压Nd-Fe-B磁环磁性能、微观组织和相结构的影响,结果表明,随着挤压速度、变形压力的提高,磁环的磁性能先增大后减小,挤压速度0.05 mm/s、变形压力164 MPa下制备的磁环磁性能最佳,剩磁、矫顽力和最大磁能积分别为12.385 kGs、10.705 kOe、32.808 MGOe。采用具有凸台结构的反向热挤压模具制备的Nd-Fe-B永磁环比常规的反向热挤压模具制备的磁环的矫顽力更高且磁性能轴向均匀性更好。
Abstract: Nd-Fe-B magnetic ring with outer diameter of 39.5 mm and wall thickness of 4.5 mm was prepared by backward hot-extrusion technology. The effects of extrusion speed, deformation pressure and mold structure on the magnetic properties, microstructure and phase structure of the backward hot-extruded Nd-Fe-B magnetic ring were studied. The results showed that, with the increase of extrusion speed and deformation stress, the magnetic properties of the magnetic ring increased first and then decreased. The magnetic properties of the magnetic ring prepared using an extrusion speed of 0.05 mm/s and a deformation pressure of 164 MPa were the best, and its remanence, coercivity and maximum magnetic energy product were 12.385 kGs, 10.705 kOe and 32.808 MGOe, respectively. The Nd-Fe-B permanent magnet prepared by the backward hot-extrusion mold with a boss structure has higher coercivity and better axial uniformity of magnetic properties than the magnetic ring prepared by the conventional backward hot-extrusion mold.
文章引用:郑立允, 杜峰, 李雅婧, 赵立新, 左思源, 赵树国, 方以坤, 左志军. Nd-Fe-B磁环反向热挤压成型工艺及性能调控[J]. 材料科学, 2024, 14(12): 1672-1680. https://doi.org/10.12677/ms.2024.1412181

参考文献

[1] Song, T., Tang, X., Yin, W., Ju, J., Wang, Z., Liu, Q., et al. (2019) Magnetic Properties Improvement of Hot-Deformed Nd-Fe-B Permanent Magnets by Pr-Cu Eutectic Pre-Diffusion Process. Acta Materialia, 174, 332-341. [Google Scholar] [CrossRef
[2] Shao, B., Cai, W. and Yang, C. (2024) Electromagnetic-Thermal-Mechanical Performance of Novel Interior Permanent Magnet Motor. Case Studies in Thermal Engineering, 63, Article ID: 105259. [Google Scholar] [CrossRef
[3] Tang, M., Bao, X., Zhou, Y., Lu, K., Li, J. and Gao, X. (2020) Microstructure and Annealing Effects of NdFeB Sintered Magnets with Pr-Cu Boundary Addition. Journal of Magnetism and Magnetic Materials, 505, Article ID: 166749. [Google Scholar] [CrossRef
[4] 陈红升, 董创辉, 董生智. 烧结辐向整体稀土永磁环的研究进展[J]. 粉末冶金工业, 2024, 34(5): 129-139.
[5] 王誉, 辛博, 朱明刚, 等. 辐射取向整体Nd-Fe-B永磁环的研究现状及发展[J]. 稀土, 2022, 43(5): 124-141.
[6] Zhu, M. and Li, W. (2017) Texture Formation Mechanism and Constitutive Equation for Anisotropic Thermorheological Rare-Earth Permanent Magnets. AIP Advances, 7, Article ID: 056236. [Google Scholar] [CrossRef
[7] Yoshikawa, N., Iriyama, T., Yamada, H., Kasai, Y. and Panchanathan, V. (1999) Radially Oriented High Energy Product Nd-Fe-B Ring Magnets. IEEE Transactions on Magnetics, 35, 3268-3270. [Google Scholar] [CrossRef
[8] 胡新建, 郭朝晖, 潘伟, 等. 内禀矫顽力Hcj对Nd-Fe-B磁体温度稳定性的影响[J]. 金属功能材料, 2004, 11(2): 1-4.
[9] Li, A.H., Li, W., Lai, B., Wang, H.J., Zhu, M.G. and Pan, W. (2010) Investigation on Microstructure, Texture, and Magnetic Properties of Hot Deformed Nd-Fe-B Ring Magnets. Journal of Applied Physics, 107, 09A725. [Google Scholar] [CrossRef
[10] Lai, B., Li, Y., Wang, H., Li, A., Zhu, M. and Li, W. (2013) Quasi-Periodic Layer Structure of Die-Upset NdFeB Magnets. Journal of Rare Earths, 31, 679-684. [Google Scholar] [CrossRef